Chemistry 221 Syllabus
Important Information

Notebook Directions
Safety Information
Additional Safety Information
Monday/Wednesday Lab Schedule
Tuesday/ Thursday Lab Schedule

Lecture Notes
You should print these out and include
them in your three-ring notebook before the scheduled lecture.

Lab 01 Melting Point (passed out in class)

Experiments (Pavia 3rd Edition)
You should print these out and include
them in your three-ring notebook.
Experiments will be posted as the semester progresses.

Lab 01 Melting Point (3rd ed.)

Experiments (Pavia 4th Edition)
You should print these out and include
them in your three-ring notebook.
Experiments will be posted as the semester progresses.

Lab 01 Melting Point (4th ed.)

Experiment Notes
You should view these before the experiment.
You need to have Macromedia Shockwave Installed to view some of the slide shows that I have put together.
Material Safety Data Sheets
 MSDS
Lab 01 Melting Point
 Melting Point Video
Preparation of Cap. Tube
(Note that you need about 1-2 mm of sample, not 0.5 inches...)
Lab 02 Solubility
 Solubility Demonstation
Examples of Different Solubilities from JCE
Lab 03 Recrystallization
 Recrystallization Movie
Note that this is a general demonstration. The recrystallization that we will perform in lab will involve triphenylmethanol and 2-propanol (aka isopropanol)
Lab 05 Refractometer
 Refractometer Use
Lab 06 GC
 Operation of the GC
Lab 07 TLC
 TLC Movie
Infrared Spectroscopy
 Tacoma Narrows Bridge
NMR
 NMR Transitions
NMR Chemical Shifts
Useful Links

Spectral Database
MSDS at Alfa Aesar
MSDS at Fischer
MSDS at SIRI
MSDS at Cornell University
MSDS from JT Baker
O-Chem Online
Online Organic Text-Carey
Java Molecular Drawing Tool